Inflection Point Engineering Hydroprocessing Operations Guide

Emergency Procedures

Chapter from the Hydroprocessing Operations Guide.

HYDROPROCESSING EMERGENCY PROCEDURES

Emergency Response Frameworks

Emergency Immediate Action Secondary Action Key Parameters to Monitor Do NOT Typical Cause Recovery
Loss of Feed Maintain H2 circ at reduced rate Reduce heater firing Close feed block valve Stabilize reactor temps Monitor for temperature excursions Prepare for shutdown if extended Reactor temperatures Recycle gas flow Separator levels Do NOT lose H2 circulation Do NOT leave heater at full fire Pump trip, upstream upset, blocked line Re-establish feed slowly when available Watch for exotherms on feed introduction
Loss of Recycle Gas Emergency shutdown heater Maintain MU H2 if possible Begin controlled depressuring Alert operations to potential H2 starvation Monitor reactor ΔTs for runaway Reactor temperatures System pressure All bed thermocouples Do NOT continue firing heater Do NOT delay response Compressor trip, suction valve close, motor failure Restore compressor Slow pressuring and heat-up Resulfide if extended outage
Loss of Makeup H2 Continue recycle gas at max rate Reduce throughput 30-50% Reduce severity (lower T) Monitor H2 purity decay Prepare for shutdown if H2 drops below limit Recycle gas H2 purity H2 consumption vs supply Product quality Do NOT maintain full throughput Do NOT increase temperature H2 plant upset, PSA failure, supply line issue Restore H2, increase throughput gradually
Excessive Temperature Rise Maximize quench to affected bed Reduce heater outlet temperature Reduce feed rate If uncontrolled: emergency depressure Do NOT delay if T exceeds metallurgical limit Individual bed temperatures Rate of temperature increase Peak temperature vs. limit Do NOT wait to see if it stabilizes Do NOT close quench valves Feed contaminant, catalyst bed issue, channeling Root cause investigation before restart May need catalyst replacement
H2S Breakthrough Reduce severity (lower WABT) Reduce feed rate Increase H2/oil ratio Sample products for sulfur Check if catalyst is exhausted (EOR) Product sulfur Recycle gas H2S All bed thermocouples Do NOT increase temperature (may worsen breakthrough) End of run, feed upset, catalyst poison Address root cause May indicate catalyst change needed
Power Failure Emergency procedures per unit SOP Emergency diesel for critical systems Maintain H2 if steam-driven compressor Check all pump status Verify emergency cooling Prepare for safe park or shutdown Everything — DCS backup critical Reactor temperatures Separator levels Do NOT forget to verify instrument air Do NOT neglect cooling systems Utility failure, grid issue, local fault Systematic restart per procedure Check all equipment before restarting

Source: Hydroprocessing_Ops_Guide_v1.xlsx · sheet “Emergency Procedures”