Inflection Point Engineering Hydroprocessing Operations Curriculum

Module 8 - Turnaround Scope

Module from the Hydroprocessing Operations Curriculum curriculum.

TURNAROUND SCOPE — CATALYST CHANGEOUT & REACTOR INSPECTION · Learning Objectives · 1. Plan and execute catalyst unloading (vacuum and gravity methods) 2. Conduct reactor vessel and internals inspections during turnaround 3. Supervise catalyst reloading to achieve target density and level 4. Complete reactor closure and leak testing 5. Manage turnaround schedule for reactor work · Catalyst Changeout — Activity Sequence

Activity Duration (days) Crew Required Equipment Safety Requirements Deliverables
Unit shutdown and cool-down 2-3 Operations (4-6) N/A Normal shutdown procedure, O2 monitoring Shutdown log, temperature records
Inert and wash (N2/steam) 1-2 Operations (4) N2 supply, steam Confined space prep, atmospheric monitoring Purge records, gas-free certificate
Reactor head removal 0.5-1 Riggers (4), mechanics (4) Crane, torque tools, head stand Crane lift plan, confined space entry permit Reactor open for inspection
Catalyst unloading (vacuum) 2-5 per reactor Catalyst crew (6-8), vacuum truck operator Vacuum truck, hoses, nitrogen lance Pyrophoric material handling, respiratory protection, inert atmosphere Spent catalyst drums (weighed), unloading report
Reactor internals inspection 1-2 Inspector (2), FOS advisor UT gauge, borescope, camera, measuring tools Confined space entry, LOTO, fall protection Inspection report: UT readings, visual findings, photos
Internals maintenance/replacement 1-5 (as needed) Mechanics (4-6), welders Welding equipment, new internals if needed Hot work permit (if welding), confined space Repair records, weld inspection reports
Catalyst loading (dense) 3-7 per reactor Catalyst crew (8-12), crane operator Dense loading equipment (Densicat), hopper, crane Confined space, dust monitoring, respiratory protection Loading report: quantities, densities, levels per bed
Reactor closure 0.5-1 Mechanics (4), torque crew Torque wrenches, new gaskets, studs Bolting procedure per PCC-1, stud verification Torque records, gasket log
Pressure test 0.5-1 Operations + inspection Test pump, pressure gauges, N2 supply Test procedure per B31.3, safety perimeter Test record (signed)
Commission and startup 5-10 Full crew Per startup procedure Full PSSR before hydrocarbon introduction Startup log, PSSR checklist
Catalyst Loading Quality Control
Parameter Target Tolerance Measurement Method Corrective Action Notes
Loaded Density Per vendor spec (typically 42-52 lb/ft³) ±2 lb/ft³ Weigh each drum loaded ÷ bed volume Re-level, add/remove catalyst Dense loading achieves 10-15% higher density than sock loading
Bed Level Level within ±1 inch across reactor diameter ±1 inch Laser level or string line measurement at 8+ points Re-level before next bed Critical for distribution — uneven level causes channeling
Catalyst Quantity Per BOM (Bill of Materials) ±0.5% of specified weight Drum count × average drum weight Reconcile with vendor, adjust grading if needed Track cumulative weight vs plan throughout loading
Catalyst Integrity No broken extrudates, dust, or contamination <1% fines by visual inspection Visual check of each drum before loading, screen at hopper Reject damaged drums, notify vendor Fines increase ΔP and reduce performance
Inert Ball Layers Per loading diagram (size graduation per spec) Correct size at each layer Verify ball size matches diagram before placing Replace incorrect size Bottom: large → small (upward); Top: small → large (upward)
Temperature (catalyst in drums) <120°F Max 150°F for safe handling IR thermometer on drums Cool drums before loading if hot, check for self-heating Presulfided catalyst can self-heat — monitor closely
Source: FOS Chief Files — Catalyst & Loading folder, Hydro Loadings, Catalyst_Loading_Best_Practices_v1.xlsx, Catalyst_Loading_Report_Template_v1.docx

Source: Hydroprocessing_Operations_Curriculum_v1.xlsx · Sheet: Module 8 - Turnaround Scope