Hydroprocessing Operations Curriculum
Module from the Hydroprocessing Operations Curriculum curriculum.
TURNAROUND SCOPE — CATALYST CHANGEOUT & REACTOR INSPECTION · Learning Objectives · 1. Plan and execute catalyst unloading (vacuum and gravity methods) 2. Conduct reactor vessel and internals inspections during turnaround 3. Supervise catalyst reloading to achieve target density and level 4. Complete reactor closure and leak testing 5. Manage turnaround schedule for reactor work · Catalyst Changeout — Activity Sequence
| Activity | Duration (days) | Crew Required | Equipment | Safety Requirements | Deliverables |
|---|---|---|---|---|---|
| Unit shutdown and cool-down | 2-3 | Operations (4-6) | N/A | Normal shutdown procedure, O2 monitoring | Shutdown log, temperature records |
| Inert and wash (N2/steam) | 1-2 | Operations (4) | N2 supply, steam | Confined space prep, atmospheric monitoring | Purge records, gas-free certificate |
| Reactor head removal | 0.5-1 | Riggers (4), mechanics (4) | Crane, torque tools, head stand | Crane lift plan, confined space entry permit | Reactor open for inspection |
| Catalyst unloading (vacuum) | 2-5 per reactor | Catalyst crew (6-8), vacuum truck operator | Vacuum truck, hoses, nitrogen lance | Pyrophoric material handling, respiratory protection, inert atmosphere | Spent catalyst drums (weighed), unloading report |
| Reactor internals inspection | 1-2 | Inspector (2), FOS advisor | UT gauge, borescope, camera, measuring tools | Confined space entry, LOTO, fall protection | Inspection report: UT readings, visual findings, photos |
| Internals maintenance/replacement | 1-5 (as needed) | Mechanics (4-6), welders | Welding equipment, new internals if needed | Hot work permit (if welding), confined space | Repair records, weld inspection reports |
| Catalyst loading (dense) | 3-7 per reactor | Catalyst crew (8-12), crane operator | Dense loading equipment (Densicat), hopper, crane | Confined space, dust monitoring, respiratory protection | Loading report: quantities, densities, levels per bed |
| Reactor closure | 0.5-1 | Mechanics (4), torque crew | Torque wrenches, new gaskets, studs | Bolting procedure per PCC-1, stud verification | Torque records, gasket log |
| Pressure test | 0.5-1 | Operations + inspection | Test pump, pressure gauges, N2 supply | Test procedure per B31.3, safety perimeter | Test record (signed) |
| Commission and startup | 5-10 | Full crew | Per startup procedure | Full PSSR before hydrocarbon introduction | Startup log, PSSR checklist |
| Catalyst Loading Quality Control | |||||
| Parameter | Target | Tolerance | Measurement Method | Corrective Action | Notes |
| Loaded Density | Per vendor spec (typically 42-52 lb/ft³) | ±2 lb/ft³ | Weigh each drum loaded ÷ bed volume | Re-level, add/remove catalyst | Dense loading achieves 10-15% higher density than sock loading |
| Bed Level | Level within ±1 inch across reactor diameter | ±1 inch | Laser level or string line measurement at 8+ points | Re-level before next bed | Critical for distribution — uneven level causes channeling |
| Catalyst Quantity | Per BOM (Bill of Materials) | ±0.5% of specified weight | Drum count × average drum weight | Reconcile with vendor, adjust grading if needed | Track cumulative weight vs plan throughout loading |
| Catalyst Integrity | No broken extrudates, dust, or contamination | <1% fines by visual inspection | Visual check of each drum before loading, screen at hopper | Reject damaged drums, notify vendor | Fines increase ΔP and reduce performance |
| Inert Ball Layers | Per loading diagram (size graduation per spec) | Correct size at each layer | Verify ball size matches diagram before placing | Replace incorrect size | Bottom: large → small (upward); Top: small → large (upward) |
| Temperature (catalyst in drums) | <120°F | Max 150°F for safe handling | IR thermometer on drums | Cool drums before loading if hot, check for self-heating | Presulfided catalyst can self-heat — monitor closely |
| Source: FOS Chief Files — Catalyst & Loading folder, Hydro Loadings, Catalyst_Loading_Best_Practices_v1.xlsx, Catalyst_Loading_Report_Template_v1.docx |
Source: Hydroprocessing_Operations_Curriculum_v1.xlsx · Sheet: Module 8 - Turnaround Scope
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