Inflection Point Engineering Hydroprocessing Operations Curriculum

Module 2 - Reactor Design

Module from the Hydroprocessing Operations Curriculum curriculum.

REACTOR DESIGN & INTERNALS · Learning Objectives · 1. Describe fixed-bed reactor configurations (single-bed, multi-bed, stacked) 2. Identify reactor internal components and their functions 3. Understand quench zone design and mixing efficiency requirements 4. Recognize common reactor problems (maldistribution, channeling, hot spots) 5. Specify inspection requirements for reactor internals during turnarounds · Reactor Internal Components

Component Function Design Criteria Common Problems Inspection Points Materials
Inlet Distributor Evenly distribute feed + H2 across reactor cross-section Flux variation <5% across bed, liquid/gas co-current downflow Plugging, erosion, uneven flow, drip point blockage Visual inspection, flow test, drip point count 316 SS or Alloy 825 (sour service)
Vapor/Liquid Distributor Tray Redistribute liquid between beds after quench mixing Bubble cap or chimney tray, 100+ distribution points per m² Tray damage from catalyst dumping, seal leg flooding Level check, cap inspection, weir height 316 SS or 321 SS
Quench Zone / Mixing Chamber Mix cold quench H2 with hot reactor effluent between beds ΔT variation <10°F across next bed inlet, mixing efficiency >95% Insufficient mixing (radial ΔT >20°F), quench nozzle erosion Thermocouple survey post-startup, nozzle inspection 316 SS, Alloy 625 quench pipe
Catalyst Support Grid Support catalyst bed weight, allow effluent to pass Support full bed weight + surge loads, screen opening sized to retain catalyst Grid deflection, screen tearing, catalyst migration Deflection measurement, screen integrity, weep holes clear Carbon steel grid, 316 SS screen
Thermocouple Bundle Monitor bed temperatures at multiple radial and axial positions Minimum 3 radial positions per bed (center, mid, wall), 2-4 axial per bed Broken TCs, incorrect location, slow response Verify all TCs reading, compare redundant readings 316 SS thermowell, Type K TC
Outlet Collector Collect treated product from bottom of last bed, direct to outlet nozzle Sized for full flow without excessive ΔP, screen to retain catalyst Plugging, erosion at high velocity points Visual inspection, screen integrity 316 SS or CS with SS screen
Scallop Screens (if radial flow) Contain catalyst in radial-flow reactor while allowing flow through Slot width sized to retain smallest catalyst particle (typically 0.5mm) Plugging with fines, erosion, buckling Slot measurement, straightness check, attachment welds Profile wire (316 SS or Alloy)
Reactor Configurations
Configuration Description Typical Service Advantages Disadvantages Typical Pressure (psig)
Single-Bed One catalyst bed, no quench Naphtha HDT, light feed treating Simple, low cost, easy catalyst change No temperature control within bed, limited severity 300-600
Multi-Bed with Quench 2-5 catalyst beds separated by quench zones Diesel HDT, VGO HDT Temperature control per bed, higher conversion capability More complex internals, quench H2 consumption 500-1500
Stacked-Bed (Series Flow) Multiple reactors in series, same H2 loop Hydrocracking, deep HDS Independent catalyst systems, flexible reactor staging Higher cost, more equipment, complex operation 1500-3000
Two-Stage Hydrocracking Stage 1: HDN/HDS, Stage 2: Cracking with clean feed Maximum conversion hydrocracking Cleaner Stage 2 feed → longer catalyst life, higher conversion Two reactor loops, H2 separation between stages, expensive 2000-3000
Counter-Current (upflow/downflow) Treat feed in last bed first (reverse flow concept) Deep ULSD desulfurization H2S removal between stages improves equilibrium for deep HDS Complex, limited commercial installations 500-1000
Source: FOS Chief Files — Hydroprocessing Design Manual, Example Calcs-Hydro, Reactor_Inspection_Reporting_Tool_v1.xlsx

Source: Hydroprocessing_Operations_Curriculum_v1.xlsx · Sheet: Module 2 - Reactor Design